Synthesis and Characterization of Nanoscale Fe3O4 by in situ Sonochemical Assisted Chemical Co-Precipitation

• DOI: https://doi.org/10.22533/at.ed.3174162407066

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• Abstract: The research of Fe3O4 nanoparticles using sonochemical-assisted chemical co-precipitation has been carried out. Synthesis had precursors ferric and ferrous at room temperature is the highlight for this research . The study aimed to improve the conventional co-precipitation method with the help of ultrasound technology. It reached the formation of small spherical and reduction of particle agglomeration by using sonochemical assisted chemical co-precipitation. This nanoparticle was characterized using X-ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FTIR). The magnetic nanoscale synthesized by sonochemical-assisted chemical coprecipitation, sonicated at 800 W 20 kHz for 30 min, had small spherical nanoparticles whose size range was 8 nm. And, the sample synthesized by conventional co-precipitation was 12 nm.